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  • Application Note

    Transport of Nanoparticles From Coated Surfaces Through Physical Contact

    This work investigated the transfer of Ag and CuO nanoparticles from consumer products via simulated dermal contact by using textile wipes as a surrogate using PerkinElmer’s NexION ICP-MS single particle analyzer with the unique Syngistix Nano Application software module for data collection and analysis

  • Application Note

    Analysis of Impurities in Nickel with Avio 500 ICP-OES Following London Metal Exchange Guidelines

    The London Metal Exchange (LME) issues specifications for a variety of purities for different metals. This work focuses on the analysis of contaminants in nickel with PerkinElmer’s Avio? 500 ICP Optical Emission Spectrometer (ICP-OES), using “Special Contract Rules for Primary Nickel” as a guideline for the analytes and required concentrations.

  • Application Note

    Analysis of Single-Walled Carbon Nanotubes with SP-ICP-MS

    Measuring the amount of metals in CNTs presents a challenge. High levels can be measured directly in the solid by several techniques, including XRF and TEM, while low-level analysis requires complete digestion of the sample prior to analysis by ICP-OES or ICP-MS.

  • Application Note

    Analysis of In-Service Oils Following ASTM D5185 with the Avio 500 ICP-OES

    Globally, heavy machinery is used in construction, mining, and a variety of other areas. As the scale of the operations increase, the size, complexity, and cost of the equipment also increase, meaning that breakdowns can be costly, both in equipment repair and lost revenue. As a result, preventive maintenance is paramount. Lubricants are among the key fluids that can be tested, especially the oil used in engines. By monitoring the elemental concentration of the oil or other lubricants (hydraulics, transmission, gear), the status of that compartment can be determined.

  • Flyer

    NexSAR HPLC-ICP-MS Speciation Solution

    Speciation studies can provide comprehensive information regarding ion mobility, bioavailability, and toxicity. Consequently, many modern labs are expanding their analytical portfolio to include HPLC-ICP-MS. For such studies, it is advantageous to have an intuitive, user-friendly system that meets the user requirements for automation, ultra-low baseline, powerful integration, and flexible data export. And no one offers a more integrated, versatile, and inert speciation solution than PerkinElmer - accelerate your speciation analysis with the NexSAR? HPLC-ICP-MS Speciation Solution.

  • Application Note

    Analysis of Wastewaters Following US EPA 200.7 Using the Avio 500 ICP-OES

    This work focuses on the analysis of wastewaters following the guidelines provided in U.S. EPA Method 200.7. The U.S. Environmental Protection Agency (EPA) developed Method 200.7 for the determination of metals and trace elements in waters and wastes by ICP-OES, with the current version being Revision 4.4.1 While the scope of this method allows it to be applied to a variety of sample types, a common application is wastewater analysis.

  • Application Note

    Microwave Digestion - EPA Method 3052 on the Multiwave 3000

    Microwave sample preparation provides an efficient and clean sample preparation for multi-element analytical techniques such as ICP-OES and ICP-MS. As Microwave assisted digestion has evolved, so have the methodologies. EPA method 3052 is designed for the “total” analysis in a variety of matrices including soil, sediments, sludge, oils, biological and botanical materials. This method is the most versatile and has been well proven. It allows variations in reagents and methodology, making it ideal for a variety of matrices and elements. The variability of this method also requires a basic understanding of digestion chemistry.

  • Brochure

    OilExpress 4 Oil Condition Monitoring System

    The OilExpress 4 system adapts to your laboratory’s needs, from dozens to thousands of samples per day. Its modular design makes it possible to scale up your sample throughput or separately utilize the oil dilution capabilities in busy laboratories that are using ICP analysis. The system minimizes your operational costs by reducing instrument downtime, increasing throughput to reduce cost per sample, and offering significant savings from decreased solvent waste.

  • Application Note

    Meeting the Challenges of Soil Analysis with the Avio 200 ICP-OES

    The analysis of soils for elemental contents presents challenges during the sample preparation step. A common method for preparing a soil sample for inorganic elemental analysis involves digesting the soil sample in an acid that is heated to near-boiling to extract the elements for analysis. When using open vessels in heating blocks, this extraction method typically takes four hours or more to complete. The sample must then be centrifuged or filtered to remove solid particles prior to analysis. The use of a microwave digestion system can speed this up significantly by completing the acid digestion in less than 50 minutes.

  • Flyer

    OilPrep 4 Oil Diluter Flyer

    Need flexible sample preparation for wear metals and particle count analyses? The OilPrep? 4 is a dedicated four-tip oil diluter that automatically dilutes oil samples with kerosene (V-Solv? ICP solvent), in preparation for wear metals and particle counting/sizing analyses by inductively coupled plasma (ICP-OES) and single particle optical sizing (SPOS), such as with the Avio? ICP-OES and LPC 500? Liquid Particle Counter.

    Some key benefits include:

    • • High throughput – Significantly improves productivity and efficiency versus manual or single-tip systems. Diluting up to 250 samples per hour, one OilPrep 4 oil diluter can prepare approximately 2000 samples in 8 hours.
    • • Flexibility – Innovative Varispan? technology provides automatic computer-controlled variable sample probe spacing for multi-tipped processing of original sample containers.
    • • Time Savings – Unlike alternate technologies, PerkinElmer’s Ultrasonic Liquid Level Sensing is not impacted by individual sample viscosities, color, or external lighting.

    Download the flyer to discover more.

  • Application Note

    Characterization of TiO2 Nanoparticle Release from Fabrics By Single Particle ICP-MS

    In the textile industry, the use of titanium dioxide (TiO2) nanoparticles (NPs) is increasing due to their ability to provide UV protection, increase the hydrophilic nature of fabrics, provide antibacterial characteristics, and reduce odors. This work demonstrates the ability of PerkinElmer's NexION® Single Particle ICP-MS with Syngistix Nano Application Software Module to both detect and measure TiO2 nanoparticles released from textiles.

  • Flyer

    5 Tips to Improving Your Sample Digestion

    Sample preparation is one of the most critical steps in your analytical process. Often accounting for 60% of your analytical timetable, it has a fundamental impact on laboratory throughput and analytical performance. Any errors within the sample preparation process will undermine the quality of your food data at all subsequent stages of your analysis. Here are five tips to improving your sample digestion for food samples.

  • Application Note

    Analysis of Cerium Dioxide Nanoparticles in Soil Using Single Particle ICP-MS

    This work demonstrates a robust method using SP-ICP-MS technology to detect CeO2 NPs which were extracted from soil samples with tetrasodium pyrophosphate (TSPP). Over the past few decades, engineered nanoparticles (ENPs) have been increasingly used in many commercial products. As a result, more and more ENPs have been released into the environment, which raises concerns over their fate, toxicity and transport therein.

  • Application Note

    Accurate Sizing and Precise Counting of 10 nm Gold Nanoparticles using the NexION 2000 ICP-MS

    In this work, we demonstrate that PerkinElmer's NexION? 2000 ICP-MS, with its unique RF generator and ion optics, coupled with the Syngistix? Nano Application Software Module, can be used to accurately measure and characterize NP sizes of 10 nm and smaller, both alone and in a mixture of NPs of various sizes.

  • Application Note

    Testing and Validation of Various Antacids for Elemental Impurities using the NexION 2000 ICP-MS

    The United States Pharmacopeia (USP) has announced that its new standards for elemental impurities in drug products has been implemented since January 1, 2018. General Chapters <232> and <2232> specify the list of elements and their permissible daily exposure (PDE) limits based on the route of administration.

  • Application Note

    Quantification of Nanoparticle Uptake into Cancer Cells using Single Cell ICP-MS

    Nanoparticles (NPs) have been of significant interest over the last two decades as they offer attractive benefits for drug delivery to overcome limitations in conventional chemotherapy. Nanoparticles can be engineered to carry both drugs and imaging probes to simultaneously detect and treat cancer. They may also be designed to specifically target diseased tissues and cells in the body. A number of nanoparticlebased cancer therapeutics have been approved for clinical use and/or are currently under development.

  • Application Note

    Analysis of In-Service Oils Following ASTM D5185 with the Avio 200 ICP-OES

    With heavy machinery, it is important to assess its status during operation to prevent breakdowns and costly repairs. A key aspect is monitoring the status of the oil or lubricants used to lubricate various components such as engines, transmissions, gearboxes and many other important areas: if the oil degrades too much or becomes highly contaminated, it can damage various components. Because of its importance, ASTM created a method for the analysis of in-service oils: method D5185.

  • Application Note

    Analysis of Oil Additives Following ASTM D4951 with the Avio 200 ICP-OES

    When blending base oils and additives for use as lubricants, it is important to know and control the concentrations of certain elements for optimal performance and longer engine life. This work will focus on the analysis of additives in new oils using PerkinElmer’s Avio? 200 ICP Optical Emission Spectrometer (ICP-OES), which overcomes limitations of other ICP-OES systems and X-ray analyses.

  • Application Note

    The Application of ASTM Standard D7720 to Used Oil Data Using TIBCO Spotfire?

    The importance of managing and utilizing such data is emphasized by the creation of ASTM standard D7720, Statistically Evaluating Measurand Alarm Limits when Using Oil Analysis to Monitor Equipment and Oil for Fitness and Contamination. This application note demonstrates the transformation of used oil data in accordance with the aforementioned ASTM standard using data visualization software program TIBCO Spotfire?.

  • Application Note

    Analysis of Soils and Waters in Accordance with U.S. EPA Method 6020B using the NexION 2000 ICP-MS

    Through the years, both industry and analytical instrumentation have advanced. With the development of new chemicals and processes, new pollutants may enter the environment. However, the capabilities of analytical instruments have also increased, allowing the measurement of ever lower levels of environmental contaminants, as well as new pollutants.

  • Case Study

    Colorado School of Mines Uses a NexION 300Q ICP-MS to Obtain a Better Understanding of the Environmental Impact of Engineered Nanomaterials

    One of the leading academic research groups involved with the study of the impact of ENPs on the environment is the Colorado School of Mines (CSM), based in Golden, Colorado.

  • Application Note

    Analysis of Drinking and Natural Waters using the NexION 2000 ICP-MS

    This work has demonstrated the ability of the NexION 2000 ICP-MS to analyze both natural and drinking water samples in Standard (i.e. non-cell) mode, in accordance with U.S. EPA Method 200.8. Accuracy has been demonstrated through the analysis of several reference materials and spike recoveries, with stability of at least nine hours. Method detection limits allow for trace-level determinations, while the ability to selectively suppress user-defined isotopes also allows the measurement of analyte levels usually only possible by ICP-OES or Flame AA. The NexION 2000 provides a comprehensive solution to the challenge of U.S. EPA Method 200.8 and other drinking and natural water analytical requirements across the globe.

  • Application Note

    Using MSF to Resolve Difficult Interferences in Metallurgical Samples with the Avio 500 ICP-OES

    The analysis of trace metals in metallurgical matrices also presents a challenge for ICP-OES: spectral interferences. Many elements have a large number of emission lines (i.e. approximately 20,000 for iron), which increases the potential for spectral interferences. This effect is compounded in metallurgical samples, where the matrix element(s) are present at high levels due to the minimal dilutions used.

  • White Paper

    Weighing the Benefits and Risks of Nanotechnology White Paper

    There is a growing body of evidence showing that there are significant differences between some nanomaterials and their non-nanoscale counterparts. What those differences portend raises many new questions about their potential to cause harm to human health and the environment.

  • Application Note

    New Research Evaluating Cisplatin Uptake in Ovarian Cancer Cells by Single Cell ICP-MS

    Cisplatin, carboplatin, and oxaliplatin are the most widely used of platinum-based cancer chemotherapy drugs in the Western world. Cisplatin's effectiveness is due to its ability to bind to the DNA, resulting in DNA-platinum (Pt) adducts, which bend the DNA. The cells must then repair the DNA damage, otherwise DNA replication is blocked resulting in cell death. Many cancers are initially sensitive to platinum-based treatment, but patients frequently relapse with tumors displaying resistance to further cisplatin therapy.

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